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on June 14, 2010 at 7:21:41 am
CSC Division of Inorganic Chemistry Lab Bank
This wiki serves as a repository of laboratory experiments suitable for undergraduate use. If you are an instructor, you may request full access to the site, allowing you to edit experiments or add your own, and view instructor-only material. Just send an email to the wiki administrator, Scott McIndoe, and he'll be pleased to add you. Joining PBWorks automatically generates a week's worth of "how-to" emails, if you're unfamiliar with the wiki format.
Experiments
Title of Experiment
|
Level
|
Keywords |
Equipment/Techniques |
prep time/cost
|
Qualitative Analysis of an Inorganic (salt) Mixture |
200
|
identification of unknown, inorganic salts, precipitation, redox, transition metal |
no special equipment
|
?
|
The Inert Pair Effect and the Relative Stabilities of Tin(IV) and Lead(IV)
.................
A related experiment synthesizing tin iodide.
|
200
.....
200 level
|
p-block, lead, tin, inert pair effect, redox, synthesis ........
A twist to the 1968 Pass & Sutcliffe expt.
|
no special equipment
|
?
|
Synthesis and Identification of a Polyiodide Salt |
200
|
p-block, halide, titration, iodometry, synthesis |
titration equipment
|
?
|
Spectroscopic Determination of a Complex Ion's Stoichiometry: Job's Method (from Angelici, but using Fe(SCN)n) |
200 |
transition metal, UV-vis, colour, coordination compound
|
visible spectrophotometer
|
?
|
Two Spectrochemical Series: Determination of ΔO |
200
|
transition metal, colour, coordination compound, synthesis, UV-vis |
scanning visible spectrophotometer |
?
|
Linkage Isomerism in Co(NH3)5(NO2)Cl2 |
300 |
transition metal, IR spectroscopy, synthesis, coordination compound |
IR spectrometer
|
?
|
Synthetic, Structural, Kinetic and Thermodynamic Study of Mo(CO)4(PR3)2 |
300 |
transition metal, IR spectroscopy, synthesis, organometallic, symmetry, carbonyl compound |
IR spectrometer |
?
|
An experiment that does several different analyses on the synthesized compound
|
200 level
|
vis spectroscopy, polarimtery & magnetic susceptibility
|
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